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The microstructure study on the HCNP and char layers shaped in the course of the combustion from the cone calorimetry exam was executed using the scanning electron microscope ZEISS Sigma HDTM. Photographs were received under vacuum in a voltage of five kV.
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PA66 pellets and HCNP powder were being dried for four h at 100 °C just before extrusion. The FR-PA66 was prepared by twin-screw extrusion reaction inside the array of 260–270 °C. The check samples ended up manufactured employing a TTI-95G injection molding device beneath 265 °C which has a one hundred eighty r/min rotation speed. Figure six reveals the microtopography of pure PA66, HCNP, and FR-PA66. It could be seen from Determine 6c which the HCNP microspheres were dispersed extra uniformly devoid of apparent stage interfaces, plus the peeling phenomenon appeared about the surface from the microspheres (Determine 6d), indicating the terminal carboxyl groups of PA66 were being chemically bonded Together with the amino groups about the floor from the microspheres through the extrusion response, which destroyed the regularity from the surface area of the microspheres (Determine 6b, sleek surface area and no peeling phenomenon) and led to the Main–shell separation of the microspheres (Determine 6d), confirming the occurrence of the in situ loading response.